مخطط الموضوع

  • contact sheet

    e learning  


    • email addressabdallah.herizi@univ-msila.dz

    • days of work: From Tuesday toThursday from 8:00 a.m. - 5:00 p.m

    • Course information :

    Faculty : Technology
    Department : COMMON BASE ST
    students : 1st year Licence
    Course Title : TP Chimie 02
    Credit : 02
    Coefficient :01
    Duration of study : 10 weeks
    Duratio of science : 02 hours
    Block: B
    Room : Lab: 5,7,8 and 9.

  • Objectif du TP

    These practical work sessions are intended for students of the 1st year Common base, The practical work module of chemistry I are composed of five manipulations:
    1st Manipulation: General notions (Safety, Measuring tools in the Laboratory)
    2nd Manipulation: Preparation of solutions.
    3rd Manipulation: Titration Colorimetric of a strong acid by a strong base.
    4th Manipulation: Redox titration .
    5th Manipulation: Acetic acid titration .

    2

    Each practical work is accompanied by theoretical information and questions are proposed, in order to control the acquisition and assimilation of knowledge. and each manipulation is sanctioned by a report given to the teacher within a maximum period of 15 days from the date of the manipulation.

  • prerequisite

    pour les TP

    So that the student will be able to provide regular work in this course, it is necessary to acquire certain prior knowledge, in particular like:


  • Plan globale

    les chapitres

  • Espace de communication avec votre enseignant

  • chapitre

  • 1st Manipulation: General notions (Safety, Measuring tools in the Laboratory)

    Working in a chemical laboratory requires the application of a certain number of safety rules; these rules are essential for the organization of work in a laboratory. When you enter the lab room for the first time, the student must know what to do, know how to dress and behave during a lab session, know the essential rules for handling equipment and chemicals, glassware commonly used and knowing how to write a report.

    TOPIC: Lab Safety AIM: How do we practice safety in the science laboratory?  DO NOW: Why is it important to follow safety rules? - ppt downloadHazard Symbols – Department of Chemistry

    The chemical laboratory exposes students to risks due both to potentially toxic chemicals and to the materials used, which an experimenter must know to use them without danger. You must therefore be aware of the risks involved and do everything to protect others and yourself, while keeping in mind that the danger can come from others.

  • 2nd Manipulation: Preparation of solutions.

    The precise of volumes measurement is a great importance in the laboratory. It can be carried out using a volumetric or graduated pipette, a graduated burette or a volumetric flask. We will show in this sequence how to prepare or dilute a solution using a volumetric flask to contain a precise volume of liquid.

    How To Prepare Solutions - YouTube


  • 3rd Manipulation:Titration Colorimetric of a strong acid by a strong base.

    In everyday life, we regularly use acidic or basic solutions: descaler, vinegar, lemon juice, ammonia, soda, etc. An acid is strong if its reaction with water can be considered complete and only its conjugate base remains in solution. The reaction of this strong acid AH is then written as follows:
    AH + H2O → A - + H3O+

    Titrage ou dosage ? | Lelivrescolaire.fr

    The goal of any titration is to determine the unknown concentration (via amount of product) of one (titrated) species using another (titrant) species of known concentration. The equivalence point between the quantities of materials present and those introduced allows, after a few calculations, the determination of the concentration of the species sought. Several methods are possible to determine this equivalence point: the introduction of a colored indicator, the pH value, the conductance value of the solution.

  • Manipulation N°4 : Redox titration


    The purpose of redox titration is to determining the normality of a reducing solution knowing that of the oxidizing solution. We propose to study the oxidation of the Fe2+ ion by the permanganate ion MnO4 - in an acid medium. This assay is called manganimetry. The oxidizing properties of the permanganate ion are at the origin of manganimetry. The oxidizing form MnO4 - is purple, the reducing form Mn2+ is colorless, allowing the equivalent point to be determined without using color indicators.

    Types of Titration: Acid-Base, Redox, Precipitation & Complexometric

  • 5 th Manipulation : Acetic acid titration.

    Acetic acid also called eisel (alcohol) made  by acetic fermentation and used as a condiment or preservative. We will consider that vinegar is an aqueous solution of acetic acid with a density d close to 1. The purpose of this lab is to determine the degree of acidity D or (°) of a vinegar and defined as the mass of acid pure acetic or ethanoic contained in 100g of vinegar. For this, we will dose the acetic (ethanoic) acid contained in a known volume of vinegar using a strong base solution of known concentration: sodium hydroxide solution (NaOH).

    Acetic
    During the assays, it is necessary to know precisely the concentration of the titrant solution (here NaOH). However, in most cases, the concentrations of the solutions are not strictly exact because:
    • the solution is made using a solid product whose purity is not guaranteed by the manufacturer.
    • the solution is made using a product whose sampling (weighing, volume) cannot be precise.
    • the chemical composition of the solution changes over time.

    • مفتوح: Friday، 15 December 2023، 8:00 AM
      مغلق: Friday، 15 December 2023، 6:00 PM

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